Elemental analysis and thermogravimetric/differential thermal analysis
Cu3(HHTP)(THQ) nanowire black powder · Powder
EA on as-prepared and N2-filled dried samples; TG/DTA in N2 and air with 1-10 deg C min-1 heating rate.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| EA-derived sample formula | [Cu3(C18O6H6)(C6O6)(H2O)11.78(NH3CH2CH2NH3)1.59] | — | — | Text Approximate | 174 · Results and discussion · Table S2 |
| Guest molecule mass loss before about 200 deg C in N2 | ca. 20.4% | — | — | Text Approximate | 174 · Results and discussion · Figure S12 |
| Nitrogen content, as-prepared dried sample | 4.58 wt.% and 4.54 wt.% in two trials | — | two trials | SI Table Range | 6 · Table S2 · Table S2 |
| Thermal stability in air | 180 deg C | — | — | Text Rounded Reported | 174 · Results and discussion · Figure S13 |
| Thermal stability in N2 | up to approximately 300 deg C | — | — | Text Approximate | 174 · Results and discussion · Figure S12 |
| Total mass loss at 500 deg C | approximately 42.3% | — | — | Text Approximate | 174 · Results and discussion · Figure S12 |