Microscopy Morphology — Quasi Solid–Liquid Reaction Strategy to In Situ Synthesize the Conductive MOF Film with Ordered Submicron Macropores for Gas Sensing

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pure PS templates on IDE · Thin Film

PS template suspension measured by DLS; SI Figure S2.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PS DLS particle-size distribution peak	peak near 170 nm	—	visual read from logarithmic DLS axis	Figure Axis Approximate	p003 · Supporting Information · Figure S2

Cu3(HITP)2 MOF at PS on IDE intermediate · Electrode

20,000 magnification SEM of pure PS, solid HATP ligand at PS, Cu3(HITP)2 MOF at PS and final TOM-Cu3(HITP)2 film.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Dried PS template diameter by SEM	approx 170 nm	—	—	Text Approximate	p004-p005 · 2.3 Morphologies of each stage · Figure 2; Figure S2

IDE loaded with TOM-Cu3(HITP)2 film · Electrode

SEM images at 5000, 10000, 20000 and 50000 magnification; Hitachi Regulus 8100 or Hitachi S4800 at 3 kV.

Geometry: film on ceramic-based gold IDE
Context: target pristine framework film with template-derived TOM morphology
Measurement source: p003-p004 · 2.2 Morphology · Figure 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TOM-Cu3(HITP)2 film thickness	about several microns	—	—	Text Approximate	p003 · 2.2 Morphology · Figure 1e
TOM macropore interconnection	adjacent submicron macropores are interconnected	—	—	Text Qualitative	p004 · 2.2 Morphology · Figure 1d,g,h
TOM submicron macropore diameterMarked as a best value within this paper	approx 150 nm	—	slight difference in pore size	Text Approximate	p003 · 2.2 Morphology · Figure 1c,g
TOM pore-wall thickness	around 30 nm	—	—	Text Approximate	p003-p004 · 2.2 Morphology · Figure 1c,g