Complete recipeSource: Main
Route 1: Solvothermal
p002 · 2.3 Synthesis of Cu3(HHTP)2
Metal precursorsCu2(OAc)4.H2O, 17.9 mg (0.090 mmol)
Linker precursorsHHTP, 14.2 mg (0.044 mmol)
Solvents8 mL ultrapure H2O; 1.0 mL DMF added dropwise
Atmospherenot specified; capped glass vial
Temperature80
Time12
Work-upCentrifuged; washed three times with H2O, ethanol, and acetone.
ActivationDried in a vacuum oven at 80 deg C for 24 h.
Show 4 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Cu2(OAc)4.H2O | 17.9 mg (0.090 mmol) | p002 · 2.3 Synthesis of Cu3(HHTP)2 |
| Linker | HHTP | 14.2 mg (0.044 mmol) | p002 · 2.3 Synthesis of Cu3(HHTP)2 |
| Solvent | ultrapure H2O | 8 mL | p002 · 2.3 Synthesis of Cu3(HHTP)2 |
| Solvent | DMF | 1.0 mL | p002 · 2.3 Synthesis of Cu3(HHTP)2 |