Visual observation of interfacial film growth
Cu-HHTP-TCNQ thin-film reaction-time series · Thin Film
Biphasic aqueous/ethyl acetate synthesis at 0 C in argon-filled vial; comparison with HHTP-only and TCNQ-only conditions.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Black film visible | clearly visible black film after 15 min, at the latest | — | — | Text Rounded Reported | 3 · 2.1. Synthesis · Figure 1c |
| Continuously grown film area | about 5 cm2 | — | — | Text Approximate | 3 · 2.1. Synthesis |
| Film visible after reaction start | visible within 1 min at 0 C | — | — | Text Rounded Reported | 3 · 2.1. Synthesis |
| HHTP-only copper reaction control | slow formation of nonconnected MOF powder after 1 h | — | — | Text Rounded Reported | 3 · 2.1. Synthesis |
| TCNQ-only copper reaction control | TCNQ alone did not show any macroscopic reaction with copper ions | — | — | Text Qualitative | 3 · 2.1. Synthesis |
| Supporting video duration | Video V1 length 49 s; data type MPEG-4, 1280x720, 25 frames/s | — | — | Text Exact Reported | 12 · Video information · Video V1 |